Iron-Catalyzed Oxidative Amidation of Tertiary Amines with Aldehydes


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 Iron-Catalyzed Oxidative Amidation of Tertiary Amines with Aldehydes (pages 82–86)

Yuanming Li, Fan Jia and Prof. Dr. Zhiping Li

Chemistry - A European Journal

Volume 19Issue 1pages 82–86January 2, 2013

Article first published online: 3 DEC 2012 | DOI: 10.1002/chem.201203824 

http://onlinelibrary.wiley.com/doi/10.1002/chem.201203824/abstract

   

Unconventional couple: A new oxidative coupling protocol for amide bond formation has been developed (see scheme). The method provides an efficient and practical route for the synthesis of tertiary amides from readily available tertiary amines and aldehydes in the presence of a simple FeCl2catalyst. Mechanistic studies indicated that a peroxide and an iminium ion act as the reactive intermediates in this oxidative amidation.

 

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